1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

Base Information

Chemical Name:1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate
CAS No.:1271825-42-3
Molecular Formula:CHO₂*C₄₆H₄₀N₅S₄
Molecular Weight:836.139
Hs Code.:

1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

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Chemical Property of 1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

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Technology Process of 1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

There total 7 articles about 1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₁₇ClN₂S₂

: 1271825-39-8
1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-(3,4-dichlobenzyl)-N,N-dimethylmethanaminium formate

: 1271825-42-3
1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C

2.1: diethyl ether; acetone / 18 h / 25 °C

2.2: 1 h

With N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; acetone;
DOI:10.1002/cmdc.201000420

Reference yield:

: 108-98-5
thiophenol

: 1271825-39-8
1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-(3,4-dichlobenzyl)-N,N-dimethylmethanaminium formate

: 1271825-42-3
1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 25 °C

2.1: trimethylaluminum; ammonium chloride / 1,2-dichloro-benzene; toluene / 144 h / 130 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 25 - 150 °C / Molecular sieve

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 65 °C

5.1: thionyl chloride / dichloromethane / 25 - 40 °C

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C

7.1: diethyl ether; acetone / 18 h / 25 °C

7.2: 1 h

With lithium aluminium tetrahydride; thionyl chloride; trimethylaluminum; potassium carbonate; ammonium chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene;
DOI:10.1002/cmdc.201000420

Reference yield:

: 1271825-10-5
2,6-bis(phenylthio)benzamidine

: 1271825-39-8
1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-(3,4-dichlobenzyl)-N,N-dimethylmethanaminium formate

: 1271825-42-3
1-(2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)-N-((2-(2,6-bis(phenylthio)phenyl)-1H-imidazol-5-yl)methyl)-N,N-dimethylmethanaminium formate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 25 - 150 °C / Molecular sieve

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 65 °C

3.1: thionyl chloride / dichloromethane / 25 - 40 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C

5.1: diethyl ether; acetone / 18 h / 25 °C

5.2: 1 h

With lithium aluminium tetrahydride; thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1002/cmdc.201000420