mer-trans-dichloro(diethylenetriamine)(benzylamine)cobalt(III) perchlorate

Base Information

Chemical Name:mer-trans-dichloro(diethylenetriamine)(benzylamine)cobalt(III) perchlorate
CAS No.:68460-50-4
Molecular Formula:C₁₁H₂₂Cl₂CoN₄*ClO₄
Molecular Weight:439.672
Hs Code.:

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Chemical Property of mer-trans-dichloro(diethylenetriamine)(benzylamine)cobalt(III) perchlorate

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Technology Process of mer-trans-dichloro(diethylenetriamine)(benzylamine)cobalt(III) perchlorate

There total 1 articles about mer-trans-dichloro(diethylenetriamine)(benzylamine)cobalt(III) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131903-58-7,14215-59-9,15025-06-6,92273-55-7
mer-{(3-azapentane-1,5-diamine)trichlorocobalt(III)}

: 100-46-9
benzylamine

: 7646-85-7,24359-56-6
zinc(II) chloride

: 68460-50-4
mer-trans-dichloro(diethylenetriamine)(benzylamine)cobalt(III) perchlorate

: unsym-fac-cis-chloro(diethylenetriamine)bis(benzylamine)cobalt(III)tetrachlorozincate(II)

Guidance literature:: With hydrogenchloride; perchloric acid; In water; addn. of 5 equiv. of amine to suspn. of Co-complex, refluxing (2 ks), cooling, filtration, warming to 320 K, addn. of 12 M HCl and ZnCl2 (pptn. of ZnCl4(2-)), filtration, addn. of 70 % HClO4 to mother liquor; collection after 0.1 - 0.3 Ms, recrystn. (dissoln. in 0.1 M HCl, addn. of 12 M HCl and 70 % HClO4); elem. anal.;
DOI:10.1016/S0020-1693(00)89488-8