Technology Process of C52H82N12O19S
There total 5 articles about C52H82N12O19S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: oxalyl dichloride / dichloromethane / 2 h / 20 °C
1.2: 2 h / 0 °C
2.1: tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer
With
oxalyl dichloride;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja208009r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: water; potassium hydroxide / methanol / Reflux
2.1: oxalyl dichloride / dichloromethane / 2 h / 20 °C
2.2: 2 h / 0 °C
3.1: tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer
With
oxalyl dichloride; water; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja208009r
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 1.5 h / -78 - 0 °C
2.1: water; potassium hydroxide / methanol / Reflux
3.1: oxalyl dichloride / dichloromethane / 2 h / 20 °C
3.2: 2 h / 0 °C
4.1: tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer
With
oxalyl dichloride; water; potassium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/ja208009r
