(C₈H₉)(CO)3Fe(C₆H₅)

Base Information

Chemical Name:(C₈H₉)(CO)3Fe(C₆H₅)
CAS No.:110096-62-3
Molecular Formula:C₁₇H₁₄FeO₃
Molecular Weight:322.143
Hs Code.:

(C<sub>8</sub>H<sub>9</sub>)(CO)3Fe(C<sub>6</sub>H<sub>5</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₈H₉)(CO)3Fe(C₆H₅)

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Technology Process of (C₈H₉)(CO)3Fe(C₆H₅)

There total 1 articles about (C₈H₉)(CO)3Fe(C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110096-70-3
(C₈H₈)(CO)2FeC(O)C₆H₅^(1-)*Li⁽¹⁺⁾*99(C₂H₅)2O=(C₈H₈)(CO)2FeC(OLi)C₆H₅*99(C₂H₅)2O

: 368-39-8
triethyloxonium fluoroborate

: 110096-62-3
(C₈H₉)(CO)3Fe(C₆H₅)

Guidance literature:: In dichloromethane; a soln. of Et3OBF4 in CH2Cl2 was added dropwise with stirring to a soln. of Fe-complex in the same solvent at -30°C under N2 atmosphere, mixt. was stirred at -30°C for 0.5 h; solvent was removed at -50°C, residue was chromd. on Al2O3 at -20°C (eluant pentane followed by pentane/ether), recrystd. from pentane at -80°C; elem. anal.;