meso-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride

Base Information

Chemical Name:meso-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride
CAS No.:495186-07-7
Molecular Formula:C₂₆H₂₄Cl₂F₂Zr
Molecular Weight:536.603
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride

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Technology Process of meso-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride

There total 1 articles about meso-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21959-01-3,125410-70-0,125410-71-1
zirconium tetrachloride bis(tetrahydrofuran) complex

: 495185-74-5
1,2-dimethyl-3-(2-fluorophenyl)cyclopentadiene

: 495186-07-7,495186-50-0
meso-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride

: rac-bis(1,2-dimethyl-3-(2-fluorophenyl)cyclopentadienyl)zirconium dichloride

Guidance literature:: With n-butyllithium; In hexane; toluene; (Ar); dropwise addn. of a soln. of lithium compd. in hexane to a soln. of ligand in toluene at -78°C, warming to room temp., cooling to -78°C, addn. of zirconium complex, refluxing for 3 d; filtration through Celite, evapn., recrystn. (n-hexane/toluene); elem. anal.;
DOI:10.1016/S0022-328X(02)01665-0