[N-acetyl-N'-methylureato(2-)-N,N'](η(5)-pentamethylcyclopentadienyl)(triphenylphosphine-P)iridium(III) chloroform solvate

Base Information

• Chemical Name: [N-acetyl-N'-methylureato(2-)-N,N'](η(5)-pentamethylcyclopentadienyl)(triphenylphosphine-P)iridium(III) chloroform solvate
• CAS No.: 253444-56-3
• Molecular Formula: CHCl₃*C₃₂H₃₆IrN₂O₂P
• Molecular Weight: 823.222
• Mol file: 253444-56-3.mol

Synonyms:

Chemical Property of [N-acetyl-N'-methylureato(2-)-N,N'](η(5)-pentamethylcyclopentadienyl)(triphenylphosphine-P)iridium(III) chloroform solvate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [N-acetyl-N'-methylureato(2-)-N,N'](η(5)-pentamethylcyclopentadienyl)(triphenylphosphine-P)iridium(III) chloroform solvate

There total 1 articles about [N-acetyl-N'-methylureato(2-)-N,N'](η(5)-pentamethylcyclopentadienyl)(triphenylphosphine-P)iridium(III) chloroform solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

IrCl2(pentamethylcyclopentadienyl)PPh3 + N-acetyl-N'-methylurea (623-59-6) → [N-acetyl-N'-methylureato(2-)-N,N'](η(5)-pentamethylcyclopentadienyl)(triphenylphosphine-P)iridium(III) chloroform solvate (253444-56-3)

Guidance literature:

With Ag₂O; In dichloromethane; N2-atmosphere; refluxing (according to Dinger et al., J.Organometal.Chem. 526, 303 (1996); ibid. 557, 231 (1998); J.Chem.Soc.Dalton Trans. 1998,1763; filtration, evapn., recrystn. (CHCl3/Et2O, slow evapn.);

DOI:10.1107/S0108270199007581

upstream raw materials:

N-acetyl-N'-methylurea