2-p-tolyl-indol-3-one-(O-benzoyl oxime )

Base Information

• Chemical Name: 2-p-tolyl-indol-3-one-(O-benzoyl oxime )
• CAS No.: 102467-94-7
• Molecular Formula: C₂₂H₁₆N₂O₂
• Molecular Weight: 340.381
• Mol file: 102467-94-7.mol

Synonyms:

Chemical Property of 2-p-tolyl-indol-3-one-(O-benzoyl oxime )

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-p-tolyl-indol-3-one-(O-benzoyl oxime )

There total 3 articles about 2-p-tolyl-indol-3-one-(O-benzoyl oxime ) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-methylphenyl)-1H-indole (55577-25-8) → 2-p-tolyl-indol-3-one-(O-benzoyl oxime ) (102467-94-7)

Guidance literature:

With water; acetic acid; sodium nitrite; anschliessendes Behandeln mit Benzoylchlorid und wss.Natronlauge;

DOI:10.1021/jo01115a023

Reference yield:

aniline (62-53-3) → 2-p-tolyl-indol-3-one-(O-benzoyl oxime ) (102467-94-7)

Guidance literature:

Multi-step reaction with 2 steps

1: boron fluoride ether adduct

2: acetic acid; water; sodium nitrite / anschliessendes Behandeln mit Benzoylchlorid und wss.Natronlauge

With boron fluoride ether; water; acetic acid; sodium nitrite;

DOI:10.1021/jo01115a023

Reference yield:

2-diazo-1-(4-methylphenyl)ethanone (17263-64-8) → 2-p-tolyl-indol-3-one-(O-benzoyl oxime ) (102467-94-7)

Guidance literature:

Multi-step reaction with 2 steps

1: boron fluoride ether adduct

2: acetic acid; water; sodium nitrite / anschliessendes Behandeln mit Benzoylchlorid und wss.Natronlauge

With boron fluoride ether; water; acetic acid; sodium nitrite;

DOI:10.1021/jo01115a023

upstream raw materials:

2-(4-methylphenyl)-1H-indole

aniline

2-diazo-1-(4-methylphenyl)ethanone