cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylstibane molybdenum(II)

Base Information

• Chemical Name: cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylstibane molybdenum(II)
• CAS No.: 83328-23-8
• Molecular Formula: C₂₈H₂₆BrMoO₂Sb
• Molecular Weight: 692.107

Synonyms:

Chemical Property of cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylstibane molybdenum(II)

Chemical Property:

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Technology Process of cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylstibane molybdenum(II)

There total 1 articles about cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylstibane molybdenum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

tricarbonylbromo(η-cyclopentadienyl)molybdenum + tribenzylstibane (5072-92-4) → cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylstibane molybdenum(II) (83328-23-8)

Guidance literature:

In benzene; byproducts: CO; (N2), to the Mo-complex in benzene added organic compound in the same solvent, mixture heated at 50°C for 50 h; solvent removed in vac., (PhCH2)3Sb removed, filtered, evaporated in vac., extracted with pentane/toluene (5:1), cooled to -78°C; elem. anal.;

upstream raw materials:

tribenzylstibane

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