{2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid

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Chemical Name:{2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid
CAS No.:98625-48-0
Molecular Formula:C₂HF₃O₂*C₃₅H₄₄N₄O₅S₂
Molecular Weight:778.914
Hs Code.:

{2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid

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Chemical Property of {2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid

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Technology Process of {2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid

There total 1 articles about {2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

: 98625-47-9
{2-[2-(2-tert-Butoxycarbonylamino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid

: 76-05-1
trifluoroacetic acid

: 98625-48-0
{2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid

Guidance literature:: for 1h; Ambient temperature;
DOI:10.1007/BF00574212

Reference yield:

: 98625-48-0
{2-[2-(2-Amino-3-tritylsulfanyl-propionylamino)-4-methylsulfanyl-butyrylamino]-4-methyl-pentanoylamino}-acetic acid; compound with trifluoro-acetic acid

: 98625-51-5
(2-{2-[2-((2R,3S)-2-Amino-3-hydroxy-butyrylamino)-3-tritylsulfanyl-propionylamino]-4-methylsulfanyl-butyrylamino}-4-methyl-pentanoylamino)-acetic acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1,3-dicyclohexylcarbodiimide, 2) (C₂H₅)3N / 1) dioxane, CH₃CO₂H, room temperature, 20 h, 2) DMF, room temperature, 24 h

2: 93.5 percent / 1 h / Ambient temperature

With triethylamine; dicyclohexyl-carbodiimide;
DOI:10.1007/BF00574212