osmium(II)tris(5,5'-diphenyl-2,2'-bipyridine)⁽²⁺⁾

Base Information

• Chemical Name: osmium(II)tris(5,5'-diphenyl-2,2'-bipyridine)⁽²⁺⁾
• CAS No.: 102869-28-3
• Molecular Formula: C₆₆H₄₈N₆Os
• Molecular Weight: 1115.35
• Mol file: 102869-28-3.mol

Synonyms:

Chemical Property of osmium(II)tris(5,5'-diphenyl-2,2'-bipyridine)⁽²⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of osmium(II)tris(5,5'-diphenyl-2,2'-bipyridine)⁽²⁺⁾

There total 1 articles about osmium(II)tris(5,5'-diphenyl-2,2'-bipyridine)⁽²⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diammonium hexachloroosmate(IV) + 5,5'-diphenyl-2,2′-bipyridine (182319-00-2) → osmium(II)tris(5,5'-diphenyl-2,2'-bipyridine)(2+) (102869-28-3)

Guidance literature:

With ammonium hexafluorophosphate; In ethylene glycol; refluxed with a slight excess of organic compound for 6 h; cooled to 80-90°C; diluted with water; soln. of NH4PF6 added dropwise; refrigerated overnight; filtered; extracted with acetone; filtered; ethanol added; evapd.; chromy.; evapd.;

DOI:10.1021/j100408a019

upstream raw materials:

5,5'-diphenyl-2,2′-bipyridine