C₃₅H₄₁Cl₂N₇O₃

Base Information

• Chemical Name: C₃₅H₄₁Cl₂N₇O₃
• CAS No.: 1092504-43-2
• Molecular Formula: C₃₅H₄₁Cl₂N₇O₃
• Molecular Weight: 678.662
• Mol file: 1092504-43-2.mol

Synonyms:

Chemical Property of C₃₅H₄₁Cl₂N₇O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₄₁Cl₂N₇O₃

There total 7 articles about C₃₅H₄₁Cl₂N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-piperazine (109-01-3) → C35H41Cl2N7O3 (1092504-43-2)

Guidance literature:

Multi-step reaction with 4 steps

1: diethyl cyanophosphonate; triethylamine / dichloromethane / 72 h / 20 °C

2: hydrogenchloride / di-isopropyl ether; isopropyl alcohol / 15 h

3: hydrogenchloride / diethyl ether; toluene; acetonitrile / 106 h / 0 - 20 °C

4: triethylamine / dichloromethane / 2 h

With hydrogenchloride; diethyl cyanophosphonate; triethylamine; In diethyl ether; dichloromethane; di-isopropyl ether; isopropyl alcohol; toluene; acetonitrile;

Reference yield:

C13H17Cl2N3O (1092069-68-5) → C35H41Cl2N7O3 (1092504-43-2)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / di-isopropyl ether; isopropyl alcohol / 15 h

2: hydrogenchloride / diethyl ether; toluene; acetonitrile / 106 h / 0 - 20 °C

3: triethylamine / dichloromethane / 2 h

With hydrogenchloride; triethylamine; In diethyl ether; dichloromethane; di-isopropyl ether; isopropyl alcohol; toluene; acetonitrile;

Reference yield:

C26H34N4O3 (1092504-69-2) → C35H41Cl2N7O3 (1092504-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C

1.2: 48 h

2.1: triethylamine / dichloromethane / 2 h

With triethylamine; trifluoroacetic acid; In dichloromethane;

upstream raw materials:

1-methyl-piperazine

C₁₃H₁₇Cl₂N₃O

C₂₆H₃₄N₄O₃

C₁₃H₁₇Cl₂N₃O*ClH

Refernces