1-ferrocenyl-6-(4-bromophenyl)dodecamethylhexasilane

Base Information

Chemical Name:1-ferrocenyl-6-(4-bromophenyl)dodecamethylhexasilane
CAS No.:352462-71-6
Molecular Formula:C₂₈H₄₉BrFeSi₆
Molecular Weight:689.961
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-ferrocenyl-6-(4-bromophenyl)dodecamethylhexasilane

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Technology Process of 1-ferrocenyl-6-(4-bromophenyl)dodecamethylhexasilane

There total 1 articles about 1-ferrocenyl-6-(4-bromophenyl)dodecamethylhexasilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1271-15-4
lithiumferrocene

: 352462-70-5
1-chloro-6-(4-bromophenyl)dodecamethylhexasilane

: 352462-71-6
1-ferrocenyl-6-(4-bromophenyl)dodecamethylhexasilane

Guidance literature:: In tetrahydrofuran; under N2 atm. soln. ferrocenyllithium in THF was added slowly to stirredsoln. 1-chloro-6-(4-bromophenyl)dodecamethylhexasilane in THF at room t emp., react. mixt. was refluxed overnight; solvent was stripped off, residual ferrocene was removed by sublimation,residue was dissolved in Et2O, aq. NH4Cl was added, org. layer was drie d over Na2SO4 and concd., chromy. on silica using heptane-toluene (95:5)as eluent;
DOI:10.1016/S0022-328X(01)00743-4