tribromo(2,4,6-tri-tert-butylphenoxy)germane

Base Information

Chemical Name:tribromo(2,4,6-tri-tert-butylphenoxy)germane
CAS No.:97241-59-3
Molecular Formula:C₁₈H₂₉Br₃GeO
Molecular Weight:573.73
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tribromo(2,4,6-tri-tert-butylphenoxy)germane

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Technology Process of tribromo(2,4,6-tri-tert-butylphenoxy)germane

There total 1 articles about tribromo(2,4,6-tri-tert-butylphenoxy)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13450-92-5
germanium tetrabromide

: 732-26-3
2,4,6-tri-tert-butylphenoxol

: 97241-59-3
tribromo(2,4,6-tri-tert-butylphenoxy)germane

Guidance literature:: With n-butyllithium; In hexane; byproducts: LiBr, butane; addn. of n-butyl lithium to a soln. of the phenol in hexane at room temp.; refluxed for 6 h; cooling; dropwise addn. of a soln. of GeBr4 in hexane at -40°C; refluxed for 6 h;; filtration; removal of solvent; distn.; mixt. with unreacted phenol obtained (content 40-50% detected by NMR);;