(OC)3FeCH₂CCOOCH₃COCH₃CHC₆H₅

Base Information

• Chemical Name: (OC)3FeCH₂CCOOCH₃COCH₃CHC₆H₅
• CAS No.: 79123-29-8
• Molecular Formula: C₁₆H₁₄FeO₆
• Molecular Weight: 358.131
• Mol file: 79123-29-8.mol

Synonyms:

Chemical Property of (OC)3FeCH₂CCOOCH₃COCH₃CHC₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (OC)3FeCH₂CCOOCH₃COCH₃CHC₆H₅

There total 1 articles about (OC)3FeCH₂CCOOCH₃COCH₃CHC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

(η3-vinylcarbene) tricarbonyliron complex + phenyldiazomethane (908094-04-2) → (OC)3FeCH2CCOOCH3COCH3CHC6H5 (79123-29-8)

Guidance literature:

In diethyl ether; byproducts: trans-stilbene, N2; at -78°C, then the reaction mixt. is agitated at room temp. for 2 h; evapg. the solvent., extg. residue with n-hexane/diethyl ether, concg. the solvent in vac., oily product dissolved in benzene and chromd., by-product sepd. with benzene, elution with benzene/diethyl ether results pure product, elem. anal.;

DOI:10.1016/S0022-328X(00)85960-4

upstream raw materials:

phenyldiazomethane