C₃₇H₄₂O₇Si

Base Information

Chemical Name:C₃₇H₄₂O₇Si
CAS No.:1315341-22-0
Molecular Formula:C₃₇H₄₂O₇Si
Molecular Weight:626.822
Hs Code.:

C<sub>37</sub>H<sub>42</sub>O<sub>7</sub>Si

Synonyms:

Suppliers and Price of C₃₇H₄₂O₇Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₄₂O₇Si

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₃₇H₄₂O₇Si

There total 17 articles about C₃₇H₄₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315341-21-9
6-bromo-3-hydroxy-2-methoxy-4-(morpholin-4-ylmethyl)benzaldehyde

: C₃₇H₄₂O₇Si

: 1315341-22-0
C₃₇H₄₂O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: 48 h / 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere

3.2: 17 h / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 12 h / 20 °C

5.1: pyridine / dichloromethane / 120 h / 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18 h / 115 - 120 °C / Inert atmosphere

7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 12 h / 20 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere

9.1: Dess-Martin periodane / dichloromethane / 12 h / 20 °C / Inert atmosphere

10.1: potassium carbonate / 4 h / 0 °C / Inert atmosphere

11.1: sulfuric acid / acetone / 48 h / 20 °C / Inert atmosphere; Molecular sieve

12.1: Dess-Martin periodane / dichloromethane / 0.83 h / 20 °C / Inert atmosphere

13.1: tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

14.1: phenyl isocyanate; triethylamine / benzene / 36 h / 20 °C / Inert atmosphere

15.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 36 h / 20 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; benzene; 6.1: Stille coupling / 13.1: Wittig reaction;
DOI:10.1021/jo200398v

Reference yield:

: 1315341-04-8
6-bromo-3-hydroxy-4-hydroxymethyl-2-methoxy-benzaldehyde

: C₃₇H₄₂O₇Si

: 1315341-22-0
C₃₇H₄₂O₇Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere

1.2: 17 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 12 h / 20 °C

3.1: pyridine / dichloromethane / 120 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18 h / 115 - 120 °C / Inert atmosphere

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 12 h / 20 °C

6.1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere

7.1: Dess-Martin periodane / dichloromethane / 12 h / 20 °C / Inert atmosphere

8.1: potassium carbonate / 4 h / 0 °C / Inert atmosphere

9.1: sulfuric acid / acetone / 48 h / 20 °C / Inert atmosphere; Molecular sieve

10.1: Dess-Martin periodane / dichloromethane / 0.83 h / 20 °C / Inert atmosphere

11.1: tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

12.1: phenyl isocyanate; triethylamine / benzene / 36 h / 20 °C / Inert atmosphere

13.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 36 h / 20 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; benzene; 4.1: Stille coupling / 11.1: Wittig reaction;
DOI:10.1021/jo200398v

Reference yield:

: 1315341-03-7
acetic acid 2-acetoxy-5-bromo-4-formyl-3-methoxybenzyl ester

: C₃₇H₄₂O₇Si

: 1315341-22-0
C₃₇H₄₂O₇Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: water; sodium hydroxide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere

2.2: 17 h / 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 12 h / 20 °C

4.1: pyridine / dichloromethane / 120 h / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18 h / 115 - 120 °C / Inert atmosphere

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 12 h / 20 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere

8.1: Dess-Martin periodane / dichloromethane / 12 h / 20 °C / Inert atmosphere

9.1: potassium carbonate / 4 h / 0 °C / Inert atmosphere

10.1: sulfuric acid / acetone / 48 h / 20 °C / Inert atmosphere; Molecular sieve

11.1: Dess-Martin periodane / dichloromethane / 0.83 h / 20 °C / Inert atmosphere

12.1: tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

13.1: phenyl isocyanate; triethylamine / benzene / 36 h / 20 °C / Inert atmosphere

14.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 36 h / 20 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; benzene; 5.1: Stille coupling / 12.1: Wittig reaction;
DOI:10.1021/jo200398v