C₂₄H₂₁F₃N₄O₄

Base Information

Chemical Name:C₂₄H₂₁F₃N₄O₄
CAS No.:1414628-73-1
Molecular Formula:C₂₄H₂₁F₃N₄O₄
Molecular Weight:486.45
Hs Code.:

C<sub>24</sub>H<sub>21</sub>F<sub>3</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₄H₂₁F₃N₄O₄

Chemical Property:

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Technology Process of C₂₄H₂₁F₃N₄O₄

There total 5 articles about C₂₄H₂₁F₃N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1414628-38-8
C₂₄H₃₈F₃N₂O₇PSi

: 1414628-73-1
C₂₄H₂₁F₃N₄O₄

: 1414628-76-4
C₂₄H₂₁F₃N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1: lithium hexamethyldisilazane / -78 - 0 °C / Inert atmosphere

2: sodium tetrahydroborate / tetrahydrofuran / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

4: ozone; methanol / dichloromethane / -78 °C / Inert atmosphere

5: acetonitrile; 1,2-dichloro-ethane / 80 °C / Inert atmosphere

6: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; tetrabutyl ammonium fluoride; ozone; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 1: |Wittig Olefination / 6: |Wittig Olefination;
DOI:10.1016/j.tetlet.2012.09.070

Reference yield:

: 1418148-10-3
C₂₅H₃₀F₄N₂O₃Si

: 1414628-73-1
C₂₄H₂₁F₃N₄O₄

: 1414628-76-4
C₂₄H₂₁F₃N₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

2: ozone; methanol / dichloromethane / -78 °C / Inert atmosphere

3: acetonitrile; 1,2-dichloro-ethane / 80 °C / Inert atmosphere

4: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With methanol; tetrabutyl ammonium fluoride; ozone; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 4: |Wittig Olefination;
DOI:10.1016/j.tetlet.2012.09.070

Reference yield:

: 1414628-45-7
C₂₇H₃₂F₄N₂O₄Si

: 1414628-73-1
C₂₄H₂₁F₃N₄O₄

: 1414628-76-4
C₂₄H₂₁F₃N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / tetrahydrofuran / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

3: ozone; methanol / dichloromethane / -78 °C / Inert atmosphere

4: acetonitrile; 1,2-dichloro-ethane / 80 °C / Inert atmosphere

5: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; tetrabutyl ammonium fluoride; ozone; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 5: |Wittig Olefination;
DOI:10.1016/j.tetlet.2012.09.070