3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt

Base Information

Chemical Name:3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt
CAS No.:1333015-38-5
Molecular Formula:C₆H₁₅N*C₁₆H₁₈ClN₆O₆P
Molecular Weight:557.974
Hs Code.:

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Chemical Property of 3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt

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Technology Process of 3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt

There total 2 articles about 3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333015-22-7
C₁₆H₁₈ClN₆O₅P

: 121-44-8
triethylamine

: 1333015-38-5
3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt

Guidance literature:: C₁₆H₁₈ClN₆O₅P; With water; iodine; In pyridine; for 0.0833333h;

triethylamine; In methanol; water; isopropyl alcohol;
DOI:10.1021/jm2001103

Reference yield:

: 106-47-8
4-chloro-aniline

: 124930-59-2
3'-azido-3'-deoxythymidin-5'-yl H-phosphonate monoester

: 1333015-38-5
3-azido-3'-deoxythymidin-5'-yl (N-4-chlorophenyl)phosphoramidate triethylammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; chlorophosphoric acid diphenyl ester / dichloromethane / 0.08 h

2: water; iodine / pyridine / 0.08 h

With pyridine; water; iodine; chlorophosphoric acid diphenyl ester; In pyridine; dichloromethane;
DOI:10.1021/jm2001103