C₃₉H₅₄FN₅O₄Si₂

Base Information

Chemical Name:C₃₉H₅₄FN₅O₄Si₂
CAS No.:1400814-02-9
Molecular Formula:C₃₉H₅₄FN₅O₄Si₂
Molecular Weight:732.058
Hs Code.:

C<sub>39</sub>H<sub>54</sub>FN<sub>5</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:

Suppliers and Price of C₃₉H₅₄FN₅O₄Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₅₄FN₅O₄Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₅₄FN₅O₄Si₂

There total 7 articles about C₃₉H₅₄FN₅O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332623-01-4
(2R,3S)-3-(methoxymethoxy)hex-5-ene-1,2-diol

: 1400814-01-8
C₃₉H₅₄FN₅O₄Si₂

: 1400814-02-9
C₃₉H₅₄FN₅O₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

3.1: ethylmagnesium bromide / tetrahydrofuran

4.1: dimethylsulfide; sodium hydrogencarbonate; ozone / methanol; dichloromethane

5.1: dmap; triethylamine / dichloromethane

6.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 4 h / Reflux

6.2: 2 h / Reflux

With 1H-imidazole; dmap; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; dimethylsulfide; trimethylsilyl trifluoromethanesulfonate; ethylmagnesium bromide; sodium hydrogencarbonate; ozone; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2.1: Swern oxidation / 6.1: silyl Hilbert-Johnson reaction / 6.2: silyl Hilbert-Johnson reaction;
DOI:10.1271/bbb.120134

Reference yield:

: 1400813-98-0
C₃₅H₅₄O₄Si₂

: 1400814-01-8
C₃₉H₅₄FN₅O₄Si₂

: 1400814-02-9
C₃₉H₅₄FN₅O₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethylsulfide; sodium hydrogencarbonate; ozone / methanol; dichloromethane

2.1: dmap; triethylamine / dichloromethane

3.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 4 h / Reflux

3.2: 2 h / Reflux

With dmap; N,O-bis-(trimethylsilyl)-acetamide; dimethylsulfide; trimethylsilyl trifluoromethanesulfonate; sodium hydrogencarbonate; ozone; triethylamine; In methanol; dichloromethane; acetonitrile; 3.1: silyl Hilbert-Johnson reaction / 3.2: silyl Hilbert-Johnson reaction;
DOI:10.1271/bbb.120134

Reference yield:

: C₃₄H₅₂O₅Si₂

: 1400814-01-8
C₃₉H₅₄FN₅O₄Si₂

: 1400814-02-9
C₃₉H₅₄FN₅O₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane

2.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 4 h / Reflux

2.2: 2 h / Reflux

With dmap; N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; acetonitrile; 2.1: silyl Hilbert-Johnson reaction / 2.2: silyl Hilbert-Johnson reaction;
DOI:10.1271/bbb.120134