Co₃(CCl)(CO)7[P(OCH₃)2C₆H₅][P(OC₆H₄CH₃)3]

Base Information

• Chemical Name: Co₃(CCl)(CO)7[P(OCH₃)2C₆H₅][P(OC₆H₄CH₃)3]
• CAS No.: 84536-26-5
• Molecular Formula: C₃₇H₃₂ClCo₃O₁₂P₂
• Molecular Weight: 943.034
• Mol file: 84536-26-5.mol

Synonyms:

Chemical Property of Co₃(CCl)(CO)7[P(OCH₃)2C₆H₅][P(OC₆H₄CH₃)3]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Co₃(CCl)(CO)7[P(OCH₃)2C₆H₅][P(OC₆H₄CH₃)3]

There total 1 articles about Co₃(CCl)(CO)7[P(OCH₃)2C₆H₅][P(OC₆H₄CH₃)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylphosphonous acid dimethyl ester (2946-61-4) + chloromethylidynetricobalt nonacarbonyl + tri-p-tolylphosphite (620-42-8) → Co3(CCl)(CO)7[P(OCH3)2C6H5][P(OC6H4CH3)3] (84536-26-5)

Guidance literature:

With sodium diphenylketyl; In tetrahydrofuran; sequence of reacts. with P(OC6H4Me-p)3 (78%) followed by P(OMe)2Ph (64%) (addn. of soln. of sodium diphenylketyl (0.01 M soln. in THF) to equimolar mixt. of reactants in THF at room temp.);

DOI:10.1016/S0022-328X(00)86919-3

upstream raw materials:

phenylphosphonous acid dimethyl ester

tri-p-tolylphosphite