Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

Base Information

Chemical Name:Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate
CAS No.:75266-55-6
Molecular Formula:C₃₁H₄₀N₂O₆
Molecular Weight:536.668
Hs Code.:

Benzyl 4-Methyl-3-<4'β-<<<N'-<(tert-butyloxy)-carbonyl>-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

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Suppliers and Price of Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

Chemical Property:

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Technology Process of Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

There total 3 articles about Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 598-23-2
3-methyl-but-1-yne

: 75266-55-6
Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-butyllithium

2: 1) KH / 1) THF, 0 deg C, 2) room temp., 1h

With n-butyllithium; potassium hydride;
DOI:10.1021/jo01312a001

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 75266-55-6
Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-butyllithium

2: 1) KH / 1) THF, 0 deg C, 2) room temp., 1h

With n-butyllithium; potassium hydride;
DOI:10.1021/jo01312a001

Reference yield:

: 68898-89-5
N,N'-tert-Butoxycarbonyl-L-prolyl-2-(4'-hydroxyphenyl)-ethylamin

: 75266-54-5
Benzyl 4-Methyl-2-pentynoate

: 75266-55-6
Benzyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-3-pentenoate

: 75266-56-7,75266-57-8
Benzyl (Z,E)-4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>-2-pentenoate

Guidance literature:: With potassium hydride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) THF, 0 deg C, 2) room temp., 1h;
DOI:10.1021/jo01312a001