PhSCH(Sn(n-Bu)3)CH₂CH₂OCPh₃

Base Information

Chemical Name:PhSCH(Sn(n-Bu)3)CH₂CH₂OCPh₃
CAS No.:1190600-11-3
Molecular Formula:C₄₀H₅₂OSSn
Molecular Weight:699.628
Hs Code.:

PhSCH(Sn(n-Bu)3)CH<sub>2</sub>CH<sub>2</sub>OCPh<sub>3</sub>

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Chemical Property of PhSCH(Sn(n-Bu)3)CH₂CH₂OCPh₃

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Technology Process of PhSCH(Sn(n-Bu)3)CH₂CH₂OCPh₃

There total 1 articles about PhSCH(Sn(n-Bu)3)CH₂CH₂OCPh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1190600-07-7
PhSCH₂CH₂CH₂OCPh₃

: 1461-22-9
tributyltin chloride

: 1190600-11-3
PhSCH(Sn(n-Bu)3)CH₂CH₂OCPh₃

: Ph(Sn(n-Bu)3)S(CH₂)3OCPh₃

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; pentane; Schlenk technique, under Ar; at -78°C to stirred soln. of n-BuLi in hexane and tmeda in pentane, added PhSCH2CH2CH2OtBu slowly via syringe; stirred for 24 h at room temp. n-Bu3SnCl added dropwise; aq. NH4Cl4 added to suspn., aq. phase extd. with Et2O, dried over Na2SO4, filtered, evapd. solvents;not isolated, detd. by (119)Sn NMR;
DOI:10.1016/j.jorganchem.2009.05.035