(triphenyl phosphite)(triisopropyl phosphite)Cr(CO)4

Base Information

• Chemical Name: (triphenyl phosphite)(triisopropyl phosphite)Cr(CO)4
• CAS No.: 134233-29-7
• Molecular Formula: C₃₁H₃₆CrO₁₀P₂
• Molecular Weight: 682.564
• Mol file: 134233-29-7.mol

Synonyms:

Chemical Property of (triphenyl phosphite)(triisopropyl phosphite)Cr(CO)4

Chemical Property:

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Technology Process of (triphenyl phosphite)(triisopropyl phosphite)Cr(CO)4

There total 1 articles about (triphenyl phosphite)(triisopropyl phosphite)Cr(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenyl phosphite (101-02-0) + cis-(piperidine)(triisopropyl phosphite)Cr(CO)4 (134132-29-9) → (triphenyl phosphite)(triisopropyl phosphite)Cr(CO)4 (134132-35-7,134233-29-7)

Guidance literature:

In tetrahydrofuran; byproducts: piperidine; Irradiation (UV/VIS); irradn. of the Cr-compound in THF for 15 min at room temp., stirred with P(OPh)3 for 2 h; filtered over celite, removed under reduced pressure, pptd. upon addn. of cold hexane, suction filtration, recrystn. from chloroform/methanol, elem. anal.;

DOI:10.1021/om00052a031

upstream raw materials:

triphenyl phosphite

cis-(piperidine)(triisopropyl phosphite)Cr(CO)4