Zr(C₄H₂NH(2-CH₂NtBu)(5-CH₂NMe₂))(PhNCONEt₂)3

Base Information

• Chemical Name: Zr(C₄H₂NH(2-CH₂NtBu)(5-CH₂NMe₂))(PhNCONEt₂)3
• CAS No.: 1383927-47-6
• Molecular Formula: C₄₅H₆₇N₉O₃Zr
• Molecular Weight: 873.309
• Mol file: 1383927-47-6.mol

Synonyms:

Chemical Property of Zr(C₄H₂NH(2-CH₂NtBu)(5-CH₂NMe₂))(PhNCONEt₂)3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Zr(C₄H₂NH(2-CH₂NtBu)(5-CH₂NMe₂))(PhNCONEt₂)3

There total 1 articles about Zr(C₄H₂NH(2-CH₂NtBu)(5-CH₂NMe₂))(PhNCONEt₂)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

PhNC(NEt2)OH (1014-72-8) + Zr(C4H2NH(2-CH2NtBu)(5-CH2NMe2))(NEt2)2 (1383927-39-6) → Zr(C4H2NH(2-CH2NtBu)(5-CH2NMe2))(PhNCONEt2)3 (1383927-47-6)

Guidance literature:

In diethyl ether; to soln. of Zr complex in Et2O added 2 equiv. PhNC(NEt2)OH in Et2O at 0°C; stirred at room temp. for 12 h; dried in vacuo; residue recrystd. from Et2O;

DOI:10.1039/c2dt30417a

upstream raw materials:

PhNC(NEt₂)OH

Zr(C₄H₂NH(2-CH₂NtBu)(5-CH₂NMe₂))(NEt₂)2