N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine

Base Information

Chemical Name:N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine
CAS No.:42592-34-7
Molecular Formula:C₁₂H₁₇NO₂
Molecular Weight:207.272
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine

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Technology Process of N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine

There total 2 articles about N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-20-8,13054-87-0
2-aminobutanol

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 42592-34-7
N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine

Guidance literature:: In ethanol;

Reference yield:

: 42592-34-7
N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine

Guidance literature:: Entspr. Carbonylverb., entspr. Amin in Bzl. od. A.;

Reference yield:

: niobium isopropoxide

: 42592-34-7
N-(1'-hydroxy-2'-butyl)-2-hydroxyacetophenoneimine

: 2Nb⁽⁵⁺⁾*5C₁₂H₁₅NO₂^(2-)=Nb₂(C₁₂H₁₅NO₂)5

Guidance literature:: In benzene; byproducts: isopropanol; refluxing Nb compd. and Schiff base (molar ratio 2:5) in dry benzene, 110-120°C, several h; azeotropically separating isopropanol; evapn.; washing (ether); elem. anal.;