2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran⁽¹²⁾-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-6-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate)

Base Information

• Chemical Name: 2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran⁽¹²⁾-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-6-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate)
• CAS No.: 326833-33-4
• Molecular Formula: C₄₁H₄₉B₁₀N₃O₉S₃
• Molecular Weight: 932.163

Synonyms:

Chemical Property of 2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran⁽¹²⁾-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-6-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran⁽¹²⁾-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-6-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate)

There total 1 articles about 2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran⁽¹²⁾-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-6-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran(12)-2-ylmethoxy]phenyl)-1H-benzimidazol-5-yl)imino)bis[ethanol] (326833-30-1) + p-toluenesulfonyl chloride (98-59-9) → 2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran(12)-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-5-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate) (326833-32-3) + 2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran(12)-2-ylmethoxy]phenyl)-1-[(4-methylphenyl)sulfonyl]-1H-benzimidazol-6-yl)imino)bis[ethanol] bis(4-methylbenzenesulfonate) (326833-33-4)

Guidance literature:

With pyridine; In pyridine; solid TsCl added in portions to carborane soln. cooled to 0°C, kept at 5°C for 72 h; poured into ice water, crystd. within 15 min, filtered off, washed (H2O), dried (vac.); obtained as mixt.;

DOI:10.1002/1522-2675(20001108)83:11<2926::AID-HLCA2926>3.0.CO;2-6

upstream raw materials:

2,2'-((2-(4-[1,2-dicarba-closo-dodecaboran⁽¹²⁾-2-ylmethoxy]phenyl)-1H-benzimidazol-5-yl)imino)bis[ethanol]

p-toluenesulfonyl chloride

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