Technology Process of C20H27NO3
There total 11 articles about C20H27NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,2-dichloro-ethane / Reflux
2: 0 °C
3: tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate / tetrahydrofuran / 7 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate;
In
tetrahydrofuran; 1,2-dichloro-ethane;
3: Tsuji-Trost type reaction;
DOI:10.1055/s-0030-1260812
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 0 °C
2: tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate / tetrahydrofuran / 7 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate;
In
tetrahydrofuran;
2: Tsuji-Trost type reaction;
DOI:10.1055/s-0030-1260812
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate;
In
tetrahydrofuran;
for 7h;
optical yield given as %de;
regioselective reaction;
Reflux;
DOI:10.1055/s-0030-1260812