hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene

Base Information

Chemical Name:hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene
CAS No.:76853-26-4
Molecular Formula:C₁₀H₁₂O₂
Molecular Weight:164.204
Hs Code.:

hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopenta<cd>pentalene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene

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Technology Process of hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene

There total 5 articles about hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106139-22-4
C₁₀H₁₀Br₂O₂

: 65181-93-3,76853-26-4,76863-42-8
hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Heating;
DOI:10.1021/jo00379a032

Reference yield:

: 106139-20-2
5,10-dioxatetracyclo<7.2.1.0^4,11.0^6,10>dodeca-2,7-diene

: 65181-93-3,76853-26-4,76863-42-8
hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene

Guidance literature:: Multi-step reaction with 2 steps

1: 25 percent / Br₂ / CCl₄ / Ambient temperature

2: tri-n-butylstannane, 2,2'-azobisisobutyronitrile (AIBN) / toluene / 2 h / Heating

With 2,2'-azobis(isobutyronitrile); bromine; tri-n-butyl-tin hydride; In tetrachloromethane; toluene;
DOI:10.1021/jo00379a032

Reference yield:

: 106139-19-9
2-bromo-6,7-dichlorohexahydro-2,6,3,5-ethanediylidene-2H,3H-1,4-dioxacyclopentapentalene

: 65181-93-3,76853-26-4,76863-42-8
hexahydro-3,2,5-ethanylylidene-2H,3H-1,4-dioxacyclopentapentalene

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 625 °C / 4 Torr

2: 25 percent / Br₂ / CCl₄ / Ambient temperature

3: tri-n-butylstannane, 2,2'-azobisisobutyronitrile (AIBN) / toluene / 2 h / Heating

With 2,2'-azobis(isobutyronitrile); bromine; tri-n-butyl-tin hydride; In tetrachloromethane; toluene;
DOI:10.1021/jo00379a032