O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

Base Information

• Chemical Name: O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose
• CAS No.: 96961-37-4
• Molecular Formula: C₁₀₃H₈₈N₂O₂₆
• Molecular Weight: 1769.83
• Mol file: 96961-37-4.mol

Synonyms:

Chemical Property of O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

There total 2 articles about O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trityl perchlorate (16721-97-4) + O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-36-3,102046-18-4) → O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-37-4,102046-21-9)

Guidance literature:

With 2,4,6-trimethyl-pyridine; In dichloromethane; for 0.25h;

DOI:10.1007/BF01142800

Reference yield:

triphenylmethyl perchlorate + O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-36-3,102046-18-4) → O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-37-4,102046-21-9)

Guidance literature:

With pyridine; 2,4,6-trimethyl-pyridine; methanol; Yield given. Multistep reaction; 1) CH₂Cl₂, 45 min, 2);

DOI:10.1016/S0040-4020(01)96688-8

upstream raw materials:

trityl perchlorate

O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose