Technology Process of C19H18ClN3O2S2
There total 9 articles about C19H18ClN3O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium periodate / tetrahydrofuran; water
2: hydrogenchloride; sodium acetate / water
3: hydrogen; palladium(II) hydroxide / methanol / 2844.39 Torr
4: triethylamine / dichloromethane
5: sodium ethanolate / tetrahydrofuran; ethanol
6: hydrazine hydrate / ethanol; acetic acid
With
hydrogenchloride; sodium periodate; hydrogen; sodium ethanolate; sodium acetate; palladium(II) hydroxide; hydrazine hydrate; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid;
2: Mannich reaction;
DOI:10.1016/j.bmcl.2011.08.008
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen; palladium(II) hydroxide / methanol / 2844.39 Torr
2: triethylamine / dichloromethane
3: sodium ethanolate / tetrahydrofuran; ethanol
4: hydrazine hydrate / ethanol; acetic acid
With
hydrogen; sodium ethanolate; palladium(II) hydroxide; hydrazine hydrate; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2011.08.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane
2: sodium ethanolate / tetrahydrofuran; ethanol
3: hydrazine hydrate / ethanol; acetic acid
With
sodium ethanolate; hydrazine hydrate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2011.08.008
