C₅₄H₈₀O₁₄

Base Information

Chemical Name:C₅₄H₈₀O₁₄
CAS No.:1365268-35-4
Molecular Formula:C₅₄H₈₀O₁₄
Molecular Weight:953.221
Hs Code.:

C<sub>54</sub>H<sub>80</sub>O<sub>14</sub>

Synonyms:

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Chemical Property of C₅₄H₈₀O₁₄

Chemical Property:

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Technology Process of C₅₄H₈₀O₁₄

There total 13 articles about C₅₄H₈₀O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365268-31-0
C₂₂H₃₀O₃

: 1365268-34-3
C₂₇H₄₀O₇

: 1365268-35-4
C₅₄H₈₀O₁₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: n-butyllithium / tetrahydrofuran / -78 °C

1.2: -78 - 20 °C

2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

2.2: 0 °C

2.3: -78 °C

3.1: 1H-imidazole / dichloromethane / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

5.1: diisobutylaluminium hydride / dichloromethane / -78 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

7.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

8.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

8.2: -78 °C

9.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

10.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

11.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

12.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

With 1H-imidazole; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; pig liver esterase; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-46-7
C₄₀H₅₄O₅Si

: 1365268-34-3
C₂₇H₄₀O₇

: 1365268-35-4
C₅₄H₈₀O₁₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

3.2: -78 °C

4.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

5.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

6.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

7.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

With hydrogenchloride; dmap; pig liver esterase; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-44-5
C₂₃H₃₀O₄

: 1365268-34-3
C₂₇H₄₀O₇

: 1365268-35-4
C₅₄H₈₀O₁₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

1.2: 0 °C

1.3: -78 °C

2.1: 1H-imidazole / dichloromethane / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

4.1: diisobutylaluminium hydride / dichloromethane / -78 °C

5.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

6.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

7.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

7.2: -78 °C

8.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

9.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

10.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

11.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

With 1H-imidazole; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; pig liver esterase; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.058