Technology Process of C28H30N8O3
There total 6 articles about C28H30N8O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; potassium phosphate; 2-Picolinic acid / dimethyl sulfoxide / 85 °C / Sealed tube
2: hydrogenchloride / water / 0 °C / Inert atmosphere
With
2-Picolinic acid; hydrogenchloride; potassium phosphate; copper(l) iodide;
In
water; dimethyl sulfoxide;
DOI:10.1002/anie.201205369
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium iodide; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 22 h / 110 °C / Inert atmosphere; Sealed tube
2: sodium cyanoborohydride; acetic acid / 20 °C / Inert atmosphere; Cooling with ice
3: sodium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere
4: copper(l) iodide; potassium phosphate; 2-Picolinic acid / dimethyl sulfoxide / 85 °C / Sealed tube
5: hydrogenchloride / water / 0 °C / Inert atmosphere
With
2-Picolinic acid; hydrogenchloride; potassium phosphate; copper(l) iodide; sodium cyanoborohydride; sodium carbonate; acetic acid; sodium iodide; N,N`-dimethylethylenediamine;
In
1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/anie.201205369
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium cyanoborohydride; acetic acid / 20 °C / Inert atmosphere; Cooling with ice
2: sodium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere
3: copper(l) iodide; potassium phosphate; 2-Picolinic acid / dimethyl sulfoxide / 85 °C / Sealed tube
4: hydrogenchloride / water / 0 °C / Inert atmosphere
With
2-Picolinic acid; hydrogenchloride; potassium phosphate; copper(l) iodide; sodium cyanoborohydride; sodium carbonate; acetic acid;
In
water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/anie.201205369