Phosphorothioic acid O-[3-(hydroxymethyl)-4-nitrophenyl]O,O-dimethyl ester

Base Information

Chemical Name:Phosphorothioic acid O-[3-(hydroxymethyl)-4-nitrophenyl]O,O-dimethyl ester
CAS No.:59417-73-1
Molecular Formula:C9H12 N O6 P S
Molecular Weight:293.23
Hs Code.:
Mol file:59417-73-1.mol

Synonyms:3-Hydroxymethylfenitrothion;Hydroxymethylfenitrothion

Suppliers and Price of Phosphorothioic acid O-[3-(hydroxymethyl)-4-nitrophenyl]O,O-dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Phosphorothioic acid O-[3-(hydroxymethyl)-4-nitrophenyl]O,O-dimethyl ester

Chemical Property:

Vapor Pressure:2.89E-07mmHg at 25°C
Boiling Point:404.4°C at 760 mmHg
Flash Point:198.4°C
PSA：135.64000
Density:1.463g/cm³
LogP:3.15700

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphorothioic acid O-[3-(hydroxymethyl)-4-nitrophenyl]O,O-dimethyl ester

There total 3 articles about Phosphorothioic acid O-[3-(hydroxymethyl)-4-nitrophenyl]O,O-dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 142827-41-6
carbomethoxyfenitrothion

: 59417-73-1
O,O-dimethyl O-<3-(hydroxymethyl)-4-nitro>phenyl phosphorothioate

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;
DOI:10.1021/jf00039a044

Reference yield:

: 54812-31-6
O,O-dimethyl O-(3-carboxy-4-nitro)phenyl phosphorothioate

: 59417-73-1
O,O-dimethyl O-<3-(hydroxymethyl)-4-nitro>phenyl phosphorothioate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / various solvent(s) / 0 °C

2: 74 percent / LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jf00039a044