1H-Imidazole-1-carboxylic acid, 1-methyl-2-propenyl ester

Base Information

• Chemical Name: 1H-Imidazole-1-carboxylic acid, 1-methyl-2-propenyl ester
• CAS No.: 141037-05-0
• Molecular Formula: C8H10N2O2
• Molecular Weight: 166.18
• Mol file: 141037-05-0.mol

Synonyms:1H-Imidazole-1-carboxylic acid 1-methyl-2-propen-1-yl ester Heller-Sarpong;(+/-)-but-3-en-2-yl 1-imidazolecarboxylate;

Chemical Property of 1H-Imidazole-1-carboxylic acid, 1-methyl-2-propenyl ester

Chemical Property:

• Refractive Index: n20/D1.482
• Flash Point: >110℃
• PSA: 44.12000
• Density: 1.092 g/mL at 25 °C
• LogP: 1.44230

Purity/Quality:

95% ^*data from raw suppliers

3-Buten-2-yl 1H-imidazole-1-carboxylate 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-1-carboxylic acid, 1-methyl-2-propenyl ester

There total 1 articles about 1H-Imidazole-1-carboxylic acid, 1-methyl-2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-hydroxy-3-butene (598-32-3) + 1,1'-carbonyldiimidazole (530-62-1) → (+/-)-but-3-en-2-yl 1-imidazolecarboxylate (141037-05-0)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 17h; Inert atmosphere;

DOI:10.1021/ol1018882

Reference yield: 87.0%

(+/-)-but-3-en-2-yl 1-imidazolecarboxylate (141037-05-0) + 2-(4-bromophenyl)-acetic acid (1878-68-8) → (+/-)-but-3-en-2-yl 2-(4-bromophenyl)acetate (1344736-06-6)

Guidance literature:

With pyridinium triflate; In acetonitrile; at 40 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol300339q

Reference yield:

Benzeneselenol (645-96-5) + (+/-)-but-3-en-2-yl 1-imidazolecarboxylate (141037-05-0) → C11H12O2Se (1047680-04-5)

Guidance literature:

In 1,2-dichloro-ethane; for 4h; Molecular sieve; Reflux; Inert atmosphere;

DOI:10.1039/b806949b

upstream raw materials:

2-hydroxy-3-butene

1,1'-carbonyldiimidazole

Downstream raw materials:

C₁₁H₁₂O₂Se

1-(1-methyl-allyl)-1H-imidazole

(+/-)-but-3-en-2-yl 2-(4-bromophenyl)acetate

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