C₂B₁₀H₁₀(C₆H₄C₂B₁₀H₁₁)2

Base Information

Chemical Name:C₂B₁₀H₁₀(C₆H₄C₂B₁₀H₁₁)2
CAS No.:620927-32-4
Molecular Formula:C₁₈H₄₀B₃₀
Molecular Weight:580.846
Hs Code.:

C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>(C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>B<sub>10</sub>H<sub>11</sub>)2

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Chemical Property of C₂B₁₀H₁₀(C₆H₄C₂B₁₀H₁₁)2

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Technology Process of C₂B₁₀H₁₀(C₆H₄C₂B₁₀H₁₁)2

There total 1 articles about C₂B₁₀H₁₀(C₆H₄C₂B₁₀H₁₁)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 20644-12-6
1,12-dicarbora-closo-dodecaborane

: 71482-44-5
1,2-bis(4-iodophenyl)-ortho-carborane

: copper(l) chloride

: 620927-31-3
H(C₂B₁₀H₁₀C₆H₄)2I

: 620927-32-4
C₂B₁₀H₁₀(C₆H₄C₂B₁₀H₁₁)2

: [1,2-C₂B₁₀H₁₀-1,4-C₆H₄-1,12-C₂B₁₀H₁₀-1,4-C₆H₄]3

Guidance literature:: With n-C₄H₉Li; In pyridine; 1,2-dimethoxyethane; hexane; (N2); p-carborane in DME stirred at room temp., BuLi in hexanes added, pyridine added after 5 min, CuCl added after 5 min, stirred at room temp.for 1 h, heated to 60°C for 15 min, 1,2-bis(4-iodophenyl)-o-carb orane added, refluxed for 3 d; cooled, dild. with ether, filtered after 20 h, the soln. washed with dil. hydrochloric acid and H2O, dried, evapd., warmed with cyclohexane contg. EtOAc, chromd. (silica, the same solvent);
DOI:10.1016/S0022-328X(03)00313-9