Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester

Base Information

Chemical Name:Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester
CAS No.:115363-64-9
Molecular Formula:C₂₇H₄₇N₄O₉PSi₂
Molecular Weight:658.836
Hs Code.:

Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester

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Technology Process of Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester

There total 1 articles about Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69504-00-3
N⁶-Benzoyl-5'-O-(monomethoxytrityl)adenosine

: 115363-50-3
2',3'-bis-O-(tert-butyldimethylsilyl)uridine 5'-O-(β-cyanoethyl N,N-diisopropylphosphoramidite)

: C₈₅H₁₁₇N₁₁O₂₂P₂Si₄

: 115363-64-9
Phosphoric acid (2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester bis-(2-cyano-ethyl) ester

: 115363-68-3
C₄₅H₈₂N₅O₁₄PSi₄

Guidance literature:: With 1H-tetrazole; 2,4,6-trimethyl-pyridine; water; iodine; Multistep reaction. Title compound not separated from byproducts; 1.) THF, RT, 45 min, 2.) 5 min;
DOI:10.1021/jo00251a010