O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine

Base Information

• Chemical Name: O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine
• CAS No.: 68405-97-0
• Molecular Formula: C₇₀H₇₉N₅O₂₄
• Molecular Weight: 1374.42

Synonyms:

Chemical Property of O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine

There total 2 articles about O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O5-[O3-(N6,O4-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O4-(2-benzyloxycarbonylamino-O4,O6-cyclohexane-1,1-diyl-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine (68405-96-9) → O5-[O3-(N6,O4-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O4-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine (68405-97-0)

Guidance literature:

With acetic acid; Ambient temperature;

DOI:10.1139/v78-243

Reference yield:

O4-(O4,O6-(R)-benzylidene-2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-O5-[O3-(N6,O4-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-1D-2-deoxy-streptamine (68405-95-8) → O5-[O3-(N6,O4-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O4-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine (68405-97-0)

Guidance literature:

With acetic acid; Ambient temperature;

DOI:10.1139/v78-243

Reference yield:

O5-[O3-(N6,O4-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O4-(2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine (68405-97-0) → O5-[O3-(N6,O4-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-2-deoxy-streptamine (68405-99-2)

Guidance literature:

Multistep reaction; (i) aq. HIO₄, THF, (ii) Et₃N, MeOH;

DOI:10.1139/v78-243

upstream raw materials:

O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-O⁴-(2-benzyloxycarbonylamino-O⁴,O⁶-cyclohexane-1,1-diyl-α-D-2-deoxy-glucopyranosyl)-1D-2-deoxy-streptamine

O⁴-(O⁴,O⁶-(R)-benzylidene-2-benzyloxycarbonylamino-α-D-2-deoxy-glucopyranosyl)-O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-1D-2-deoxy-streptamine

Downstream raw materials:

O⁵-[O³-(N⁶,O⁴-(Ξ)-benzylidene-2,6-bis-benzyloxycarbonylamino-β-L-2,6-dideoxy-idopyranosyl)-β-D-ribofuranosyl]-N,N'-bis-benzyloxycarbonyl-2-deoxy-streptamine

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