(C₅(CH₃)5)Ti(C₆F₅)(CH₂B(C₆F₅)2)(OSi(CH₂CH₂Si(C₆H₅)2CH₃)3)

Base Information

• Chemical Name: (C₅(CH₃)5)Ti(C₆F₅)(CH₂B(C₆F₅)2)(OSi(CH₂CH₂Si(C₆H₅)2CH₃)3)
• CAS No.: 852447-90-6
• Molecular Formula: C₇₄H₆₈BF₁₅OSi₄Ti
• Molecular Weight: 1429.36
• Mol file: 852447-90-6.mol

Synonyms:

Chemical Property of (C₅(CH₃)5)Ti(C₆F₅)(CH₂B(C₆F₅)2)(OSi(CH₂CH₂Si(C₆H₅)2CH₃)3)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₅(CH₃)5)Ti(C₆F₅)(CH₂B(C₆F₅)2)(OSi(CH₂CH₂Si(C₆H₅)2CH₃)3)

There total 2 articles about (C₅(CH₃)5)Ti(C₆F₅)(CH₂B(C₆F₅)2)(OSi(CH₂CH₂Si(C₆H₅)2CH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(C5(CH3)5)Ti(CH3)(CH3B(C6F5)3)(OSi(CH2CH2Si(C6H5)2CH3)3) → (C5(CH3)5)Ti(C6F5)(CH3)(OSi(CH2CH2Si(C6H5)2CH3)3) (852447-91-7) + (C5(CH3)5)Ti(C6F5)(CH2B(C6F5)2)(OSi(CH2CH2Si(C6H5)2CH3)3) (852447-90-6) + methylbis(pentafluorophenyl)borane (170151-48-1)

Guidance literature:

In benzene-d6; under Ar; benzene-d6 soln. of Ti complex stored at room temp. for 96 h; not isolated; monitored by (1)H NMR spectra;

DOI:10.1021/om049010p

Reference yield:

(C5(CH3)5)Ti(CH3)2(OSi(CH2CH2Si(C6H5)2CH3)3) (852447-88-2) + tris(pentafluorophenyl)borate (1109-15-5) → dimethylpentafluorophenylborane (363596-54-7) + (C5(CH3)5)Ti(C6F5)(CH3)(OSi(CH2CH2Si(C6H5)2CH3)3) (852447-91-7) + (C5(CH3)5)Ti(C6F5)(CH2B(C6F5)2)(OSi(CH2CH2Si(C6H5)2CH3)3) (852447-90-6) + methylbis(pentafluorophenyl)borane (170151-48-1)

Guidance literature:

In benzene-d6; under Ar; in NMR tube; Ti complex and B(C6F5)3 (molar ratio 2:1) dissolved in benzene-d6 at room temp.; shaken; maintained at room temp. (296 K)for 22 h; not isolated; monitored by (1)H NMR spectra; mixt. of Ti-CH2C6F5 and Ti-Me complexes (3:97), BMe(C6F5)2 and BMe2(C6F5) obtained;

DOI:10.1021/om049010p

upstream raw materials:

(C₅(CH₃)5)Ti(CH₃)2(OSi(CH₂CH₂Si(C₆H₅)2CH₃)3)

tris(pentafluorophenyl)borate