4,5-methylenedioxy-diphenic acid dimethyl ester

Base Information

• Chemical Name: 4,5-methylenedioxy-diphenic acid dimethyl ester
• CAS No.: 145688-60-4
• Molecular Formula: C₁₇H₁₄O₆
• Molecular Weight: 314.295
• Mol file: 145688-60-4.mol

Synonyms:

Chemical Property of 4,5-methylenedioxy-diphenic acid dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5-methylenedioxy-diphenic acid dimethyl ester

There total 2 articles about 4,5-methylenedioxy-diphenic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenanthro[3,2-d][1,3]dioxole-5,6-dione (109512-33-6) → 4,5-methylenedioxy-diphenic acid dimethyl ester (145688-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran; methanol; aqueous hydrogen peroxide / anschliessend Erwaermen mit wss. Kalilauge

2: methanol; diethyl ether

With tetrahydrofuran; methanol; diethyl ether; dihydrogen peroxide;

DOI:10.1007/BF00901772

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 6-(2-carboxy-phenyl)-benzo[1,3]dioxole-5-carboxylic acid (64511-19-9) → 4,5-methylenedioxy-diphenic acid dimethyl ester (145688-60-4)

Guidance literature:

With methanol; diethyl ether;

DOI:10.1007/BF00901772

upstream raw materials:

diazomethane

6-(2-carboxy-phenyl)-benzo[1,3]dioxole-5-carboxylic acid

phenanthro[3,2-d][1,3]dioxole-5,6-dione