2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle

Base Information

Chemical Name:2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle
CAS No.:137021-97-7
Molecular Formula:C₁₃H₁₆OS₂
Molecular Weight:252.401
Hs Code.:

Synonyms:

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Chemical Property of 2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle

Chemical Property:

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Technology Process of 2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle

There total 6 articles about 2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36797-15-6
phenyl dithioacetate

: 137021-97-7,137022-08-3
2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / 1.) LDA / 1.) THF, -78 degC, 15 min, 2.) 1 min

2: 1.) LDA / 1.) THF, -78 degC, 20 min, 2.) -78 degC, 45 min

3: 72 h

With lithium diisopropyl amide;
DOI:10.1016/S0040-4020(01)86559-5

Reference yield:

: 36797-15-6
phenyl dithioacetate

: 137021-97-7,137022-08-3
2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / 1.) LDA / 1.) THF, -78 degC, 15 min, 2.) 1 min

2: 1.) LDA / 1.) THF, -78 degC, 20 min, 2.) -78 degC, 45 min

3: 72 h

With lithium diisopropyl amide;
DOI:10.1016/S0040-4020(01)86559-5

Reference yield:

: 137021-71-7
3-hydroxybutanedithioate de phenyle

: 137021-97-7,137022-08-3
2-(1-hydroxyethyl)-pent-4-enedithioate de phenyle

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, -78 degC, 20 min, 2.) -78 degC, 45 min

2: 72 h

With lithium diisopropyl amide;
DOI:10.1016/S0040-4020(01)86559-5