C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

Base Information

Chemical Name:C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2
CAS No.:890881-66-0
Molecular Formula:C₇₄H₇₀Cl₂O₂P₄Rh₂S₂
Molecular Weight:1456.11
Hs Code.:

C<sub>6</sub>H<sub>4</sub>[(SCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)RhCl(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>5</sub>)]2

Synonyms:

Suppliers and Price of C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

There total 2 articles about C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆H₄[(SC₂H₄P(C₆H₅)2)Rh(P(C₆H₅)2C₂H₄OC₆H₅)]2⁽²⁺⁾*2B(C₆F₅)4^(1-)=C₆H₄[(SC₂H₄P(C₆H₅)2)Rh(P(C₆H₅)2C₂H₄OC₆H₅)]2(B(C₆F₅)4)2

: 1112-67-0
tetrabutyl-ammonium chloride

: 890881-66-0
C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

Guidance literature:: In dichloromethane-d2; treatment of C6H4(SCH2CH2PPh2RhPPh2CH2CH2OC6H5)2(B(C6F5)4)2 with stoich.amts. of N(C4H9)4Cl in CD2Cl2;
DOI:10.1021/om0602310

Reference yield:

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 205743-54-0
1,4-bis(2-diphenylphosphanylethoxy)-2,3,5,6-tetramethylbenzene

: 162616-45-7
Ph₂P(CH₂)2OPh

: 890881-66-0
C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

Guidance literature:: In dichloromethane; treatment of 1,4-(Ph2PCH2CH2O)2C6Me4 and Ph2PCH2CH2OC6H5 with (Rh(COD)Cl)2 in CH2Cl2;
DOI:10.1021/om0602310

Reference yield:

: 890881-66-0
C₆H₄[(SCH₂CH₂P(C₆H₅)2)RhCl(P(C₆H₅)2CH₂CH₂OC₆H₅)]2

: 2797-28-6
lithium tetrakis(pentafluorophenyl)borate

: C₆H₄[(SC₂H₄P(C₆H₅)2)Rh(P(C₆H₅)2C₂H₄OC₆H₅)]2⁽²⁺⁾*2B(C₆F₅)4^(1-)=C₆H₄[(SC₂H₄P(C₆H₅)2)Rh(P(C₆H₅)2C₂H₄OC₆H₅)]2(B(C₆F₅)4)2

Guidance literature:: In dichloromethane; treatment of C6H4(SCH2CH2PPh2RhClPPh2CH2CH2OC6H5)2 with excess of LiB(C6F5)4 in CH2Cl2; removal of remaining LiB(C6F5)4 by washing with dry benzene;
DOI:10.1021/om0602310