[Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(μ-η2-C,C':κ2S,S'-acetylenedithiolate)Pt(1,10-phenanthroline)]BPh4

Base Information

Chemical Name:[Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(μ-η2-C,C':κ2S,S'-acetylenedithiolate)Pt(1,10-phenanthroline)]BPh4
CAS No.:1207518-47-5
Molecular Formula:C₂₄H₂₀B*C₅₅H₄₇CoN₂P₃PtS₂
Molecular Weight:1466.35
Hs Code.:

Synonyms:

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Chemical Property of [Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(μ-η2-C,C':κ2S,S'-acetylenedithiolate)Pt(1,10-phenanthroline)]BPh4

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Technology Process of [Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(μ-η2-C,C':κ2S,S'-acetylenedithiolate)Pt(1,10-phenanthroline)]BPh4

There total 1 articles about [Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(μ-η2-C,C':κ2S,S'-acetylenedithiolate)Pt(1,10-phenanthroline)]BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 18432-95-6
dichloro(1,10-phenanthroline)platinum(II)

: potassium graphite

: [Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(η2-SC2SCH2Ph)]*thf

: 143-66-8
sodium tetraphenyl borate

: 1207518-47-5
[Co(I)(1,1,1-tris(diphenylphosphinomethyl)ethane)(μ-η2-C,C':κ2S,S'-acetylenedithiolate)Pt(1,10-phenanthroline)]BPh4

Guidance literature:: In tetrahydrofuran; (Ar, Schlenk technique); addn. of KC8 to thf soln. of cobalt compd. at -78°C, stirring at room temp. for 2 h, addn. of platinum compd. and then borate deriv., stirring for 18 h; evapn., chromy. (SiO2, CH2Cl2/hexane (10:1)), crystn. (CH2Cl2/hexane), elem. anal.;
DOI:10.1039/b913859e