Technology Process of 4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hexa-2t,4t-dienal-diethylacetal
There total 1 articles about 4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hexa-2t,4t-dienal-diethylacetal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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entspr. β-C(16)-Aldehyd, Tetraethoxysilan (A.) (N2, 3h, 20grad, p-TsOH, H3PO4);
- Guidance literature:
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Multi-step reaction with 2 steps
1: ZnCl2; ethyl acetate / Erwaermen des Reaktionsprodukts mit wss. Natriumacetat enthaltender Essigsaeure
2: diethyl ether; liquid NH3; ethyl magnesium bromide / Reaktion ueber mehrere Stufen
With
diethyl ether; ethylmagnesium bromide; ammonia; ethyl acetate; zinc(II) chloride;
DOI:10.1002/hlca.19560390130
- Guidance literature:
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Multi-step reaction with 4 steps
1: ZnCl2; ethyl acetate / Erwaermen des Reaktionsprodukts mit wss. Natriumacetat enthaltender Essigsaeure
2: diethyl ether; liquid NH3; ethyl magnesium bromide / Reaktion ueber mehrere Stufen
3: Lindlar-catalyst; toluene; quinoline / Hydrogenation
4: petroleum ether
With
quinoline; Lindlar's catalyst; diethyl ether; ethylmagnesium bromide; ammonia; ethyl acetate; toluene; zinc(II) chloride; Petroleum ether;
DOI:10.1002/hlca.19560390130