Co3(μ-CCl)(CO)7(μ-(AsPh2)2)O

Base Information

• Chemical Name: Co3(μ-CCl)(CO)7(μ-(AsPh2)2)O
• CAS No.: 263869-98-3
• Molecular Formula: C₃₂H₂₀As₂ClCo₃O₈
• Molecular Weight: 894.782
• Mol file: 263869-98-3.mol

Synonyms:

Chemical Property of Co3(μ-CCl)(CO)7(μ-(AsPh2)2)O

Chemical Property:

Purity/Quality:

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Technology Process of Co3(μ-CCl)(CO)7(μ-(AsPh2)2)O

There total 1 articles about Co3(μ-CCl)(CO)7(μ-(AsPh2)2)O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

chloromethylidynetricobalt nonacarbonyl + tetraphenyl-diarsane (2215-36-3) → Co3(μ-CCl)(CO)7(μ-(AsPh2)2)O (263869-98-3) + ClCCo3(CO)8As(C6H5)3

Guidance literature:

In toluene; Co-complex and As2Ph4 were dissolved in toluene, heated at 40°C with stirring for 4 h under N2; solvent was removed under vac., residue was dissolved in CH2Cl2, silicachromy. column, eluted with hexane/CH2Cl2; elem. anal.;

DOI:10.1039/a906611j

upstream raw materials:

tetraphenyl-diarsane