1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid

Base Information

• Chemical Name: 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid
• CAS No.: 129133-58-0
• Molecular Formula: C₄₃H₅₂N₆O₇
• Molecular Weight: 764.922

Synonyms:

Chemical Property of 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid

Chemical Property:

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Technology Process of 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid

There total 3 articles about 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

(Z)-3,4-dimethyl-5<(4,4-dimethyl-3-methoxycarbonylmethyl-5-oxo-pyrrolydin-2-yliden)methyl>-1H pyrrole-2-carboxylic acid tert-butyl ester (84408-31-1) + 2,7-Dimethyl-3-ethyl-9-formyl-dipyrrinon-8-(benzyloxycarbonyl-aminoethyl)-propylamid (129112-00-1) → 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid (129133-58-0)

Guidance literature:

DOI:10.1007/BF00809534

Reference yield:

2-benzyloxycarbonylaminoethylamine (72080-83-2) → 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid (129133-58-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent

2: 35 percent

DOI:10.1007/BF00809534

Reference yield:

(Z)-3-Ethyl-9-formyl-2,7-dimethyl-dipyrrin-1-one-8-propanoic acid (31402-16-1) → 1,19-Dioxo-17-ethyl-3-methoxycarbonylmethyl-2,2,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-8-(N-benzyloxycarbonyl-aminoethyl)-propylamid (129133-58-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent

2: 35 percent

DOI:10.1007/BF00809534

upstream raw materials:

(Z)-3,4-dimethyl-5<(4,4-dimethyl-3-methoxycarbonylmethyl-5-oxo-pyrrolydin-2-yliden)methyl>-1H pyrrole-2-carboxylic acid tert-butyl ester

2,7-Dimethyl-3-ethyl-9-formyl-dipyrrinon-8-(benzyloxycarbonyl-aminoethyl)-propylamid

2-benzyloxycarbonylaminoethylamine

(Z)-3-Ethyl-9-formyl-2,7-dimethyl-dipyrrin-1-one-8-propanoic acid

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