trans-bis-[1,2-bis(diphenylphosphino)ethane]-fluoro-(diazopropano)-molybdenum tetraphenylborate

Base Information

Chemical Name:trans-bis-[1,2-bis(diphenylphosphino)ethane]-fluoro-(diazopropano)-molybdenum tetraphenylborate
CAS No.:663910-08-5
Molecular Formula:C₂₄H₂₀B*C₅₅H₅₄FMoN₂P₄
Molecular Weight:1301.11
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-bis-[1,2-bis(diphenylphosphino)ethane]-fluoro-(diazopropano)-molybdenum tetraphenylborate

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Technology Process of trans-bis-[1,2-bis(diphenylphosphino)ethane]-fluoro-(diazopropano)-molybdenum tetraphenylborate

There total 1 articles about trans-bis-[1,2-bis(diphenylphosphino)ethane]-fluoro-(diazopropano)-molybdenum tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-[MoF(NNH₂)((C₆H₅)2PC₂H₄P(C₆H₅)2)2][B(C₆H₅)4]

: 143-66-8
sodium tetraphenyl borate

: 123-38-6
propionaldehyde

: 663910-08-5
trans-bis-[1,2-bis(diphenylphosphino)ethane]-fluoro-(diazopropano)-molybdenum tetraphenylborate

Guidance literature:: In dichloromethane; (MoF(NNH2)(dppe)2)(BF4) dissolved in 10 ml dichloromethane at room temp.; CH3CH2CHO added in excess; react. mixt. stirred overnight; red soln. became brown-green; filtered; 10 ml (C2H5)2O added; green solid dissolvedin 20 ml of CH3OH; NaB(C6H5)4 added; ppt. filtered, washed (methanol and hexane); dried under vac. for several hs; detd. by elem. anal.;
DOI:10.1016/S0925-8388(03)00348-7