3, 5-Diacetyl-1,2,4-trimethoxybenzene

Base Information

• Chemical Name: 3, 5-Diacetyl-1,2,4-trimethoxybenzene
• CAS No.: 13909-74-5
• Molecular Formula: C₁₃H₁₆O₅
• Molecular Weight: 252.267
• DSSTox Substance ID: DTXSID801225368
• Mol file: 13909-74-5.mol

Synonyms:3, 5-diacetyl-1,2,4-trimethoxybenzene;SCHEMBL6899605;BNWRLGCEQMYDGG-UHFFFAOYSA-N;DTXSID801225368;13909-74-5;Ethanone, 1,1a(2)-(2,4,5-trimethoxy-1,3-phenylene)bis-

Chemical Property of 3, 5-Diacetyl-1,2,4-trimethoxybenzene

Chemical Property:

• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 252.09977361
• Heavy Atom Count: 18
• Complexity: 315

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(=O)C1=CC(=C(C(=C1OC)C(=O)C)OC)OC

Technology Process of 3, 5-Diacetyl-1,2,4-trimethoxybenzene

There total 1 articles about 3, 5-Diacetyl-1,2,4-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-diacetyl-1,2,4-trihydroxybenzene (2999-24-8) + dimethyl sulfate (77-78-1) → 1,3-diacetyl-2,4,5-trimethoxy-benzene (13909-74-5)

Guidance literature:

With potassium carbonate; acetone;

Reference yield:

1,3-diacetyl-2,4,5-trimethoxy-benzene (13909-74-5) → 1,3-diacetoxy-2,4,5-trimethoxy-benzene

Guidance literature:

With peracetic acid;

Reference yield:

1,3-diacetyl-2,4,5-trimethoxy-benzene (13909-74-5) → 3-acetoxy-2,5,6-trimethoxyacetophenone (3162-47-8)

Guidance literature:

With peracetic acid; toluene-4-sulfonic acid;

DOI:10.1039/jr9650002743

upstream raw materials:

3,5-diacetyl-1,2,4-trihydroxybenzene

dimethyl sulfate

Downstream raw materials:

3-acetoxy-2,5,6-trimethoxyacetophenone