1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline

Base Information

Chemical Name:1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline
CAS No.:109566-49-6
Molecular Formula:C₁₈H₁₃N₃O
Molecular Weight:287.321
Hs Code.:

1-methoxy-5-phenyl-pyridazino[3,4-<i>c</i>]quinoline

Synonyms:

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Chemical Property of 1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline

Chemical Property:

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Technology Process of 1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline

There total 10 articles about 1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1032-67-3
N-benzoylmethylphthalimide

: 109566-49-6
1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline

Guidance literature:: Multi-step reaction with 9 steps

1: aq.-ethanolic KOH

2: SOCl₂ / Behandeln des Chlorids mit NH₃ in Benzol

3: N₂H₄+H₂O; pyridine

4: P₂O₅ / 175 °C

5: methyl magnesium iodide; benzene; diethyl ether

6: aqueous HCl

7: Diazotization_.und anschliessenden Behandeln mit wss.NaOH

8: P₂O₅; POCl₃

9: methanol

With pyridine; hydrogenchloride; methanol; potassium hydroxide; methyl magnesium iodide; thionyl chloride; diethyl ether; phosphorus pentoxide; hydrazine hydrate; trichlorophosphate; benzene;
DOI:10.1039/jr9570003722

Reference yield:

: 108718-55-4
3-amino-2-phenyl-quinoline-4-carboxylic acid amide

: 109566-49-6
1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline

Guidance literature:: Multi-step reaction with 6 steps

1: P₂O₅ / 175 °C

2: methyl magnesium iodide; benzene; diethyl ether

3: aqueous HCl

4: Diazotization_.und anschliessenden Behandeln mit wss.NaOH

5: P₂O₅; POCl₃

6: methanol

With hydrogenchloride; methanol; methyl magnesium iodide; diethyl ether; phosphorus pentoxide; trichlorophosphate; benzene;
DOI:10.1039/jr9570003722

Reference yield:

: 117440-08-1
2-phenyl-3-phthalimido-quinoline-4-carboxylic acid amide

: 109566-49-6
1-methoxy-5-phenyl-pyridazino[3,4-c]quinoline

Guidance literature:: Multi-step reaction with 7 steps

1: N₂H₄+H₂O; pyridine

2: P₂O₅ / 175 °C

3: methyl magnesium iodide; benzene; diethyl ether

4: aqueous HCl

5: Diazotization_.und anschliessenden Behandeln mit wss.NaOH

6: P₂O₅; POCl₃

7: methanol

With pyridine; hydrogenchloride; methanol; methyl magnesium iodide; diethyl ether; phosphorus pentoxide; hydrazine hydrate; trichlorophosphate; benzene;
DOI:10.1039/jr9570003722