[(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester
• CAS No.: 141018-44-2
• Molecular Formula: C₃₆H₄₄N₂O₆
• Molecular Weight: 600.755

Synonyms:

Chemical Property of [(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester

Chemical Property:

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Useful:

Technology Process of [(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester

There total 1 articles about [(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane (98760-08-8) + 1-((3aS,8aR)-2,2-Dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-3-(4-hydroxy-phenyl)-propan-1-one (141018-39-5) → [(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester (141018-44-2)

Guidance literature:

With n-butyllithium;

DOI:10.1021/jo00036a004

Reference yield:

[(1S,2S,4R)-1-Benzyl-5-((3aS,8aR)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-2-hydroxy-4-(4-hydroxy-benzyl)-5-oxo-pentyl]-carbamic acid tert-butyl ester (141018-44-2) → N-(2(R)-hydroxy-1(S)-indanyl)-5(S)-[1,1-dimethylethoxy-carbonylamino]-4(S)-hydroxy-6-phenyl-2(R)-(4-hydroxyphenylmethyl) hexanamide (138498-62-1)

Guidance literature:

With methanol; camphor-10-sulfonic acid;

DOI:10.1021/jo00036a004

upstream raw materials:

(2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane

1-((3aS,8aR)-2,2-Dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-3-(4-hydroxy-phenyl)-propan-1-one

Downstream raw materials:

N-(2(R)-hydroxy-1(S)-indanyl)-5(S)-[1,1-dimethylethoxy-carbonylamino]-4(S)-hydroxy-6-phenyl-2(R)-(4-hydroxyphenylmethyl) hexanamide

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