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Technology Process of C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2

C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2

Base Information
  • Chemical Name:C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2
  • CAS No.:96193-47-4
  • Molecular Formula:C34H36P2Ru
  • Molecular Weight:607.677
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>Ru(C<sub>2</sub>H<sub>5</sub>)P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>CH(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2
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Technology Process of C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2

There total 1 articles about C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R(Ru),R(C))-{Ru(η5-C5H5)(Cl)(prophos)}

(R(Ru),R(C))-{Ru(η5-C5H5)(Cl)(prophos)}

ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

{(C<sub>5</sub>H<sub>5</sub>)Ru(C<sub>6</sub>H<sub>5</sub>)2PCH(CH<sub>3</sub>)CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2H}

{(C5H5)Ru(C6H5)2PCH(CH3)CH2P(C6H5)2H}

C<sub>5</sub>H<sub>5</sub>Ru(C<sub>2</sub>H<sub>5</sub>)P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>CH(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2
96193-47-4

C5H5Ru(C2H5)P(C6H5)2CH2CH(CH3)P(C6H5)2

Guidance literature:
In diethyl ether; toluene; MeMgBr in ether was added to soln. of complex in toluene at 50°C, mixt. was stirred for 22 h (N2); evapd., ppt. was dissolved in toluene, filtered, slow diffusion of ether;
DOI:10.1021/om00126a012
upstream raw materials:

ethylmagnesium bromide

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