tetra-μ-2-fluorobenzoato-κ10O:O';O:O,O';O:O';O,O':O'-bis[aqua(4,4'-bipyridine-κN)(2-fluorobenzoato-κO)lanthanum(III)]

Base Information

Chemical Name:tetra-μ-2-fluorobenzoato-κ10O:O';O:O,O';O:O';O,O':O'-bis[aqua(4,4'-bipyridine-κN)(2-fluorobenzoato-κO)lanthanum(III)]
CAS No.:709030-87-5
Molecular Formula:C₆₂H₄₄F₆La₂N₄O₁₄
Molecular Weight:1460.85
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetra-μ-2-fluorobenzoato-κ10O:O';O:O,O';O:O';O,O':O'-bis[aqua(4,4'-bipyridine-κN)(2-fluorobenzoato-κO)lanthanum(III)]

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Technology Process of tetra-μ-2-fluorobenzoato-κ10O:O';O:O,O';O:O';O,O':O'-bis[aqua(4,4'-bipyridine-κN)(2-fluorobenzoato-κO)lanthanum(III)]

There total 1 articles about tetra-μ-2-fluorobenzoato-κ10O:O';O:O,O';O:O';O,O':O'-bis[aqua(4,4'-bipyridine-κN)(2-fluorobenzoato-κO)lanthanum(III)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 553-26-4
4,4'-bipyridine

: 10025-84-0,20211-76-1
lanthanum(III) chloride hexahydrate

: 445-29-4
o-fluoro-benzoic acid

: 709030-87-5
tetra-μ-2-fluorobenzoato-κ10O:O';O:O,O';O:O';O,O':O'-bis[aqua(4,4'-bipyridine-κN)(2-fluorobenzoato-κO)lanthanum(III)]

Guidance literature:: With NaOH; In ethanol; water; soln. of 2-fluorobenzoic acid (0.5 mol) (EtOH) adjusted to pH 6-7 with aq. soln. of NaOH; soln. of 4,4'-bipyridine (0.5 mol) and LaCl3*6H2O (0.5mol) (EtOH) added; mixt. heated under reflux with stirring for 2 h; ppt. filtered off; crystd. after one month at room temp.;
DOI:10.1107/S0108270103029470